Polyethylene from Ethanol/Bill of Materials: Difference between revisions
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| Line 13: | Line 13: | ||
6. High heat oven for calcination | 6. High heat oven for calcination | ||
7. Size 30-50 mesh | 7. Size 30-50 mesh | ||
8. Rotary evaporating flask | |||
==Ethanol dehydration catalyst materials== | ==Ethanol dehydration catalyst materials== | ||
Reagents: | Reagents: | ||
1. Al2O3 (gamma | 1. Al2O3 (gamma aluminum trioxide) BET SSA 200 m2/g | ||
2. Na2CO3 | 2. Na2CO3 | ||
3. Ti(SO4)2 | 3. Ti(SO4)2 | ||
| Line 25: | Line 27: | ||
TiCl4 | TiCl4 | ||
n-hexene | n-hexene | ||
Silica | |||
Isopentane | |||
Triethyl aluminum | |||
Revision as of 02:34, 18 May 2012
| Polyethylene from Ethanol | ||
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Fluid bed reactor
Information on construction materials for Fluidized bed reactor can be found on its wikipage.
Catalyst preparation equipment
Necessary equipment: 1. Laboratory scale 2. Three neck round bottom flask 3. Magnetic stirrer 4. pH meter 5. Centrifuge 6. High heat oven for calcination 7. Size 30-50 mesh
8. Rotary evaporating flask
Ethanol dehydration catalyst materials
Reagents: 1. Al2O3 (gamma aluminum trioxide) BET SSA 200 m2/g 2. Na2CO3 3. Ti(SO4)2
Ethylene polymerization catalyst materials
MgCl2 anhydrous Tetrahydrofuran TiCl4 n-hexene
Silica Isopentane
Triethyl aluminum